Abstract: To meet the urgent demand of the national “carbon peaking and carbon neutrality” strategy for talent cultivation in the materials discipline, the School of Materials Science and Engineering at Southeast University constructs a “dual carbon” oriented teaching system for the Material Analysis Experimental Course. By establishing a three-dimensional teaching content framework of “foundation-frontier-innovation,” the system integrates experimental modules in frontier fields such as new energy materials and advanced analysis technologies. It also optimizes and establishes a multi-dimensional evaluation system of “process-outcome-competence.” This reform scheme achieves deep integration of experimental teaching with cutting-edge technologies in the materials discipline, significantly enhancing students’ interdisciplinary innovative thinking, engineering practice ability, and team collaboration efficiency.