Abstract: The traditional academic and stylized training programs for postgraduate experimental teaching seriously restricts the practical ability of students.In this paper,based on the current situation of graduate students course teaching in modern chemical analysis technologyand of the cultivation of postgraduates, we take the literature of student research frontier as a new teaching content, use laboratory advanced instruments to organize students to take samples for testing, collect and analye the map, and establish teaching case (Card library).The reform teaching content and teaching method is helpful to improve the innovation consciousness of the graduate students and enhance their operation skills, and lay the foundation for the future research papers.