Abstract: To improve the teaching effect of Analytical Chemistry Experiment, several efficient reforms were applied as follows: The prolegomena was introduced into the teaching process to help students make transform from theory to experiment as soon as possible. The system of teachers’ pre-experiment integrating with students’ experimental operation was established to achieve staged and stratified teaching. Opening laboratory was used to raise student’s independent innovation ability and environmental awareness. The operation examination was adopted as the main evaluation to check students’ learning effect. All the reforms were proved to make up the traditional experimental teaching limitations and obtain preferable effects.