Abstract: Based on the current hot topic of chemistry research and our group’s longstanding interest in enaminone research, the synthesis and characterization of N-(2-hydroxylphenyl)enaminone were introduced, and the application of scientific research to undergraduate teaching was explored. This comprehensive experiment involves multi-disciplinary knowledge and experimetal techniques with practicality and operability. It can not only enrich the teaching content, but also facilitate the comprehensive training of students’ theoretical knowledge and experimental skills, stimulate students’ interest in scientific research, and cultivate students’ creative ability.