狄璐. 气态流动鼓泡发生器的研制与应用[J]. 实验科学与技术, 2024, 22(1): 16-21. DOI: 10.12179/1672-4550.20230396
引用本文: 狄璐. 气态流动鼓泡发生器的研制与应用[J]. 实验科学与技术, 2024, 22(1): 16-21. DOI: 10.12179/1672-4550.20230396
DI Lu. Development and Application of Gas Flow Bubbling Generator[J]. Experiment Science and Technology, 2024, 22(1): 16-21. DOI: 10.12179/1672-4550.20230396
Citation: DI Lu. Development and Application of Gas Flow Bubbling Generator[J]. Experiment Science and Technology, 2024, 22(1): 16-21. DOI: 10.12179/1672-4550.20230396

气态流动鼓泡发生器的研制与应用

Development and Application of Gas Flow Bubbling Generator

  • 摘要: 随着全球化石资源的不断消耗,可再生资源的转化利用已成为科研工作者的关注焦点。由生物质经过生物或化学方法转化而获得的生物基低碳醇的催化转化是近些年来研究的热点。为高效率探索多种模型催化反应,该文研制了气态流动鼓泡发生器来替代传统的固定床反应器的进料过程,目的是进行不同的模型催化反应探索实验。通过对比二者的实验结果显示,该设备具有误差小、试验快、操作简单等特点,且其设计所占空间小、便携等优点,适用于多种原位表征技术。通过将气态流动鼓泡发生器与原位漫反射红外光谱联用,使学生深入学习了红外理论知识和仪器设备的工作原理,将学生们学到的催化学科的相关基础知识进行融会贯通。气态流动鼓泡发生器不仅辅助科研实验的探索,还可拓展到实验教学的应用,提升学生的科研创新能力,为科教融合、教研一体提供了新范式。

     

    Abstract: With the continuous consumption of global fossil resources, the conversion of renewable resources has become the focus of scientific researchers. The catalytic conversion reaction of bio-based lower alcohols obtained by the biological or chemical conversion of biomass is a hot research topic in recent years. In order to efficiently explore a variety of model catalytic reactions, a gaseous flow bubbling generator is developed to replace the feeding process of the traditional fixed-bed reactor. The purpose is to carry out different model catalytic reaction exploration experiments. By comparing the experimental results of the two equipments, it is shown that the gas flow bubbling generator has the characteristics of small error, fast test and simple operation. In addition, the advantages of its small footprint and portability are just right for a variety of in-situ characterization techniques. By combining the gas flow bubbling generator with the in-situ diffuse reflection infrared spectroscopy, students are able to study the theoretical knowledge of the infrared spectroscopy and the working principles of instruments, and integrate the basic knowledge on catalysis that have learned. The gas flow bubbling generator not only assists the exploration of scientific research experiments, but also can be extended to the application of experimental teaching, which improves students’ scientific research innovation ability, and provides a new paradigm for the integration of science and education and the integration of teaching and research.

     

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